New deformation method for obtaining gradient microstructure in brass rods

Authors

  • Irina Volokitina Karaganda Industrial University, Department of Metallurgy and Materials Science, Respublika Avenue 30, 101400 Temirtau, Kazakhstan
  • Anastasia Denissova Karaganda Industrial University, Department of Metallurgy and Materials Science, Respublika Avenue 30, 101400 Temirtau, Kazakhstan
  • Gulnur Tleulessova Karaganda Industrial University, Department of Metallurgy and Materials Science, Respublika Avenue 30, 101400 Temirtau, Kazakhstan

DOI:

https://doi.org/10.14311/AP.2026.66.0456

Keywords:

radial-shear broaching, brass, rod, microstructure, drawing

Abstract

The combined deformation technology used to enhance the properties of gradient metal materials with a nanostructured surface layer has attracted significant attention due to their exceptional properties, making them highly promising for industrial applications. These materials exhibit a unique combination of high strength, ductility, and wear resistance. However, achieving the desired properties and gradient microstructure in these materials requires precise control over the deformation process. The objective of this work was to investigate the effect of combined deformation processing, integrating drawing through stationary (freely rotating) RSR mill rolls followed by die drawing, on the evolution of microstructure and the mechanical properties of initially coarse-grained alpha-brass. The laboratory experiment was conducted at a room temperature using rods with a diameter of 30 mm. The results revealed that introducing radial-shear broaching had a significant effect on the properties and microstructure of the material. The combined technological process of integrating radial-shear broaching through stationary rolls followed by die drawing, successfully produced a pronounced gradient microstructure in CuZn36 brass rods, where the grain size was refined to 1 μm in the surface zone while remaining at 20 μm at the centre. This structural refinement resulted in a symmetrical, U-shaped microhardness distribution across the cross-section, with peak values reaching 170 ± 4 HV0.1 in the heavily deformed surface layer compared to 84 ± 3 HV0.1 in the initial annealed state.

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References

[1] J. Li, Q. Mei, Y. Li, T. Wang. Production of surface layer with gradient microstructure and microhardess on copper by high pressure surface rolling. Metals 10(1):73, 2020. https://doi.org/10.3390/met10010073

[2] I. Volokitina, A. Volokitin, E. Panin, et al. Improvement of strength and performance properties of copper wire during severe plastic deformation and drawing process. Case Studies in Construction Materials 19:e02609, 2023. https://doi.org/10.1016/j.cscm.2023.e02609

[3] I. Volokitina, A. Volokitin, A. Denissova, et al. Effect of thermomechanical processing of building stainless wire to increase its durability. Case Studies in Construction Materials 19:e02346, 2023. https://doi.org/10.1016/j.cscm.2023.e02346

[4] I. Volokitina, A. Volokitin, M. Latypova, et al. Effect of controlled rolling on the structural and phase transformations. Progress in Physics of Metals 24(1):132–156, 2023. https://doi.org/10.15407/ufm.24.01.132

[5] I. Volokitina, A. Volokitin. Changes in microstructure and mechanical properties of steel-copper wire during deformation. Metallurgist 67(1):232–239, 2023. https://doi.org/10.1007/s11015-023-01510-7

[6] J. Xu, D. Li, D. Shan, B. Guo. Microstructural evolution and micro/meso-deformation behavior in pure copper processed by equal-channel angular pressing. Materials Science and Engineering A 664:114–125, 2016. https://doi.org/10.1016/j.msea.2016.03.016

[7] S. Atefi, M. H. Parsa, D. Ahmadkhaniha, et al. A study on microstructure development and mechanical properties of pure copper subjected to severe plastic deformation by the ECAP-conform process. Journal of Materials Research and Technology 21:1614–1629, 2022. https://doi.org/10.1016/j.jmrt.2022.09.103

[8] I. Volokitina. Change in the microstructure and properties of steel-aluminum wire during “ECA-pressing – drawing” process. Journal of Chemical Technology and Metallurgy 57(3):631–636, 2022.

[9] A. Volokitin, I. Volokitina, Z. Gelmanova, A. Denissova. Thermomechanical treatment influence on the copper wire microstructure evolution. Theoretical and Applied Mechanics Letters 16(2):100650, 2026. https://doi.org/10.1016/j.taml.2025.100650

[10] T. K. Akopyan, Y. V. Gamin, S. P. Galkin, et al. Radial-shear rolling of high-strength aluminum alloys: Finite element simulation and analysis of microstructure and mechanical properties. Materials Science and Engineering: A 786:139424, 2020. https://doi.org/10.1016/j.msea.2020.139424

[11] A. Naizabekov, A. Arbuz, S. Lezhnev, et al. The development and testing of a new method of qualitative analysis of the microstructure quality, for example of steel AISI 321 subjected to radial shear rolling. Physica Scripta 94(10):105702, 2019. https://doi.org/10.1088/1402-4896/ab1e6e

[12] S. P. Galkin. Regulating radial-shear and screw rolling on the basis of the metal trajectory. Steel in Translation 34(7):57–60, 2004.

[13] A. Naizabekov, I. Volokitina, A. Volokitin, E. Panin. Structure and mechanical properties of steel in the process “pressing-drawing”. Journal of Materials Engineering and Performance 28(3):1762–1771, 2019. https://doi.org/10.1007/s11665-019-3880-6

[14] I. Volokitina, B. Sapargaliyeva, A. Agabekova, et al. Study of changes in microstructure and metal interface Cu/Al during bimetallic construction wire straining. Case Studies in Construction Materials 18:e02162, 2023. https://doi.org/10.1016/j.cscm.2023.e02162

[15] G. I. Raab, D. V. Gunderov, L. N. Shafigullin, et al. Structural variations in low-carbon steel under severe plastic deformation by drawing, free torsion, and drawing with shear. Materials Physics and Mechanics 24(3):242–252, 2015.

[16] I. Volokitina, E. Panin, A. Volokitin, et al. Investigation of the stress-strain state during new combined deformation technology. Eurasian Physical Technical Journal 22(2(52)):109–120, 2025. https://doi.org/10.31489/2025N2/109-120

[17] I. Volokitina, A. Volokitin, G. Tleulessova. Obtaining copper bar graded microstructure by radial-shear and traditional drawing. Metallurgist 69(3):410–416, 2025. https://doi.org/10.1007/s11015-025-01955-y

[18] M. M. Skripalenko, B. A. Romantsev, S. P. Galkin, et al. Prediction of the fracture of metal in the process of screw rolling in a two-roll mill. Metallurgist 61(11):925–933, 2018. https://doi.org/10.1007/s11015-018-0588-z

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Published

2026-09-08

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How to Cite

Volokitina, I., Denissova, A., & Tleulessova, G. (2026). New deformation method for obtaining gradient microstructure in brass rods. Acta Polytechnica, 66(4), 456–462. https://doi.org/10.14311/AP.2026.66.0456